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Introduction to Semimicro Qualitative Analysis, 8th edition

Published by Pearson (September 30, 2004) © 2005

  • Theodore E. Brown Emeritus) University of Illinois
  • H Eugene LeMay University of Nevada, Reno
  • Bruce E. Bursten Worcester Polytechnic Institute
  • Catherine Murphy University of Illinois at Urbana-Champaign
  • Patrick Woodward The Ohio State University
  • Matthew E. Stoltzfus The Ohio State University
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For courses in General Chemistry (Lecture and Laboratory) and Qualitative Inorganic Analysis.

 

This self-teaching lab manual presents a process for learning descriptive chemistry and the chemistry of the more common elements and their compounds in the format of a scheme of analysis. Students and challenged to call upon their manipulative and observational skills to provide the basis for identifying a substance or a mixture of substances. Part I describes the strategy of qualitative analysis so that students have a review of the principles readily available when they are engaged in the details of laboratory work; Part II presents the concepts involved in qualitative analysis, systematically dealing with the nature of the chemical compounds; Part III features well-tested analytical laboratory procedures.

CONTENTS

Part I GENERAL STRATEGY

1 The Strategy of Qualitative Analysis

Summary

Part II CONCEPTS IN QUALITATIVE ANALYSIS

2 The Nature of Chemical Reactions

Kinetics

Chemical Equilibrium

Thermodynamics

Summary

3 The Nature of Chemical Compounds

Physical Properties of Compounds

Classification of Chemical compounds

The Ionization of Water

Acids and Bases

4 Solution Phenomena

Concentration Units

Solubility

Equilibrium Processes Involving Sparingly Soluble Ionic Substances

Colloidal dispersions

5 Complex Compounds

Lewis Theory of Chemical Combinations

Nomenclature

Theoretical Considerations

Stability of Complex Ions

The Role of Complex Ions in Qualitative Analysis

6 Oxidation–Reduction ReactionsPart III THE PRACTICE OF QUALITATIVE ANALYSIS

7 The Practical Aspects of Qualitative Analysis

The Periodic Table

Chemical Reactions

Equilibrium Considerations

Formation of Precipitates

Dissolving Precipitates

Laboratory Safety

8 Laboratory Practices

Summary of Laboratory Work

Record of Laboratory Work and Laboratory Reports

Laboratory Procedures

9 The Silver Group

The Chemistry of the Silver Group Ions

Precipitation and Analysis of the Silver Group

Separation of Lead from Silver and Mercury (I)

Separation and Detection of Silver and Mercury

10 The Copper-Arsenic Group

The Chemistry of the Copper-Arsenic Group Ions

Separation of the Copper Subgroup from the Arsenic Subgroup

Separation of Mercury from Lead, Bismuth, Copper, and Cadmium

Separation of Lead from Bismuth, Copper, and Cadmium

Separation of Bismuth from Copper and Cadmium

Detection of Copper and Cadmium

Separation of Arsenic from Antimony and Tin

11 The Aluminum-Nickel Group

The chemistry of the Aluminum-Nickel Group Ions

Precipitation and Analysis of the Aluminum-Nickel Group

Separation of the Aluminum Subgroup from the Nickel Subgroup

Detection of Iron, Cobalt, Nickel, and Manganese

12 The Barium-Magnesium Group

The Chemistry of the Barium-Magnesium Group Ions

Detection of Ammonium Salts

The Separation and Detection of Barium

The Separation and Detection of Calcium

Detection of Sodium and Potassium

13 The Analysis of Alloys 14 Analysis of Salts and Salt Mixtures

Examination of the Solid

Solubility of the Salt

Reactions with Specific Reagents

Preliminary Experiments

Analysis of Unknown Salt

Examination of the Solid

Dissolution of the Solid

Determine What Cations Are Present

Treatment of the Unknown with Class Reagents

Specific Tests for Anions

15 Recording and Reporting Analysis APPENDICES

I Brief Review of Oxidation Numbers

II Solution of Quadratic Equations

III Reagents and Equipment Used

Index of Procedures

Index

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